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Lead electrodeposition processes from the basic (nitrate) and complex  (acetate) electrolytes were mutually compared by the scanning electron  microscopic and the X-ray diffraction analysis of the produced powder  particles. The shape of dendritic particles strongly depended on the type of  electrolyte. The dendrites composed of stalk and weakly developed primary  branches (the primary type) were predominantly formed from the basic  electrolyte. The ramified dendrites composed of stalk and of both primary and  secondary branches (the secondary type) were mainly formed from the complex  electrolyte. In the both type of powder particles Pb crystallites were  predominantly oriented in the (111) plane. Formation of powder particles of  the different shape with the strong (111) preferred orientation was discussed  and explained by the consideration of the general characteristics of the  growth of a crystal in the electrocrystallization processes. [Projekat  Ministarstva nauke Republike Srbije, br. 172046: Electrochemical synthesis  and characterization of nanostructured functional materials for application  in new technologies

Influence of the type of electrolyte on the morphological and crystallographic characteristics of lead powder particles