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A new R2edda-type ester, diisobutyl (S,S)-2,2'-(1,2-ethane-diyldi- imino)di(4-methylpentanoate) dihydrochloride, ((S,S)-H2iBu2eddl)Cl2, 1, and its palladium(II) complex, dichloro(diisobutyl (S,S)-2,2'-(1,2-ethanediyldiimi- no)di(4-methylpentanoate))palladium(II), (PdCl2{(S,S)-iBu2eddl}), 2, were syn- thesized and characterized by elemental analysis, as well as IR and NMR spec- troscopy. It was found that complex 2 was obtained as mixture of two diaste- reoisomers, observed in NMR spectra. The crystal structure of compound 1 was determined by X-ray diffraction studies and is described. The isolated crystals consisted of one dicationic species ((S,S)-H2iBu2eddl) 2+ and two Cl - .

journal of the serbian chemical society

Palladium(II) complexes with R2edda derived ligands, Part III: Diisobutyl (s,s)-2,2'-(1,2-ethanediyldiimino)di(4-methylpentanoate) and its palladium(II) complex: Synthesis and characterization