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The sigmaNiMo( Al) phase was formed using Ni3Al/Mo diffusion couples at 1423,  1473 and 1523 K. The growth of formed phase and the concentration-distance  profiles for each component in the diffusion couples were examined by  electron probe microanalysis (EPMA). The activation energy for the parabolic  growth of σ phase is found to be 525.3 kJ/mol. The concentration dependence  and average ternary interdiffusion coefficients in single σ-NiMo(Al) phase  were calculated, and the Arrhenius equations of the D for the σ-NiMo(Al)  phase are calculated, the diffusional interaction between Ni, Mo and Al in  σ-NiMo(Al) phase was studied by the crossinterdiffusion coefficients.  Moreover, these results were utilized to explain the σ phase formation and  growth in γ’ phase

Interdiffusion behavior in sigma-phase using Ni3Al/Mo diffusion couples