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Synthesis of an unconventional resin based on 4-vinylpyridine (4-VP) and its   Cu(II) sorption behavior were studied. Three samples of macroporous   crosslinked poly(4-vinylpyridine-co-ethylene glycol dimethacrylate) [P4VPE]   with different porosity parameters were prepared by suspension   copolymerization by varying the n-heptane amount in the inert component. The   samples were characterized by mercury porosimetry, elemental analysis and   x-ray photoelectron spectroscopy (XPS). The sorption of P4VPE for Cu(II)   ions, determined under non-competitive conditions, was relatively rapid, i.e.   the maximum capacity was reached within 30 min. The maximum experimental   sorption capacity for the sample with the highest values of pore diameter and   specific pore volume (Sample 3, Qeq = 89 mg g-1) was 17.5 times higher than   for the sample with the lowest values of pore diameter and specific pore   volume (Sample 1, Qeq = 5.1 mg g-1). Since the values for pyridine content in   all P4VPE samples were almost the same, it was concluded that the porosity   parameters have predominant influence on Cu(II) sorption rates on P4VPE. The   sorption behavior and the rate-controlling mechanisms were analyzed using six   kinetic models (pseudo-first order, pseudo-second order, Elovich,   intraparticle diffusion, Bangham and Boyd models). XPS study clarified the   nature of the formed P4VPE-Cu(II) species. [Projekat Ministarstva nauke   Republike Srbije, br. TR 37021 i br. III 43009

Cu(II) immobilization onto a one-step synthesized poly(4-vinylpyridine-co-ethylene glycol dimethacrylate) resin: Kinetics and XPS analysis