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Distillation is a process in which miscible liquids are separated based on their physical properties, specifically, relative volatilities. A liquid can be classified as volatile when it is readily vaporized at a relatively low temperature. The boiling of the more volatile components of the mixture drives the distillation process. When the vapor is cooled, the more volatile material condenses in a greater proportion than the less volatile material. It is a unit operation in which constituents of liquid mixture are separated by using thermal energy depends upon the relative volatility of constituents by partial vaporization and condensation. Distillation with rectification or Fractional distillation gives almost pure product. The product removed from top is called the distillate or overhead product and that removed from the bottom is called the bottom product. This unit operation is also termed as fractional distillation or fractionation.

Overview of Distillation Techniques and Process in Recovery and Reuse of Volatile Liquids