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We have studied the quasi-binary phase diagram along the line of NdBa2Cu3Oy and BaCuO2 in 1%O2+Ar. In this study, the nucleation and melt of NdBa2Cu3Oy in Ba-rich solvent were observed in situ using a laser-scanning microscope under 1%O2+Ar. The liquidus and solidus lines of nearly stoichiometric Nd123 were constructed. Phase identification has been performed on the samples quenched from the reaction temperatures determined by differential thermal analyses through X-ray powder diffraction measurements and scanning electron microscopy.

teion kougaku/teion kōgaku

Properties and Applications of Bulk High Temperature Superconductors. Phase Diagram of Nd-Ba-Cu-O System in a Reduced Oxygen Atmosphere Studied by Laser Scanning Microscopy.