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The phases which precipitate from solutions of thorium nitrate and hydrofluoric acid or sodium fluoride have been studied. Variables investigated include ratios of Na:F:Th, pH, temperature, and time in contact with the mother liquor. Twelve phases were observed to form. The structure of one phase, Na/sub 2/ThF/sub 6/, (space group P anti 62m; Z = 1; a = 6.14A; c = 3.696A.) is proposed. The structure of 6-carbomethoxy-1-thioniabicyclodecane iodide is also reported (space group P2/sub 1//n; Z = 4; a = 8.890A; b = 20.120A; c = 8.150A; ..beta.. = 110.17/sup 0/).

Crystallographic studies of sodium thorium fluoride precipitates and of a thioniabicyclo compound. [6-carbomethoxy-1-thioniabicyclodecane iodide]