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We have demonstrated a new technique capable of detecting generalized corrosion of metallographically-polished materials with nanometer-scale precision. After exposing a lithographically-patterned coupon of Alloy 22 to an electrolyte in a potentiostatically-controlled cell for twenty-four hours, we detected the loss of up to 130nm of metal. In addition, ''wormholes'' were detected at certain points of intersection of three grain boundaries

Demonstration of lithographic patterning in measurements of general and localized corrosion on alloy 22