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A combination of cryogenic electron microscopy and cryogenic focused ion beam enabled the characterization of the interface between Li metal and lithium phosphorous oxynitride, one of the well-known interfaces to exhibit exemplary electrochemical stability with a lithium metal anode. The probed structural and chemical information leads to a more comprehensive understanding of the underlying cause for the interfacial stability and its formation mechanism.

Unveiling the Stable Nature of the Solid Electrolyte Interphase between Lithium Metal and Lipon Via Cryogenic Electron Microscopy