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We present a calibration for attenuated total reflectance (ATR) micro-FTIR for analysis of H 2 O in hydrous glass. A Ge ATR accessory was used to measure evanescent wave absorption by H 2 O within hydrous rhyolite and other standards. Absorbance at 3450 cm -1  (representing total H 2 O or H 2 Ot) and 1630 cm -1  (molecular H 2 O or H 2 Om) showed high correlation with measured H 2 O in the glasses as determined by transmission FTIR spectroscopy and manometry.

american mineralogist

Amorphous Materials: Properties, structure, and durability. Analysis of H 2 O in silicate glass using attenuated total reflectance (ATR) micro-FTIR spectroscopy