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The structural phase transition of the titanomagnetite (Fe 3-x Ti x O 4 ) solid solution under pressures up to 60 GPa has been clarified by single-crystal and powder diffraction studies using synchrotron radiation and a diamond-anvil cell. Present Rietveld structure refinements of the solid solution prove that the prefered cation distribution is based on the crystal field preference rather than the magnetic spin ordering in the solid solution.

High-pressure phase transitions of Fe 3–x Ti x O 4 solid solution up to 60 GPa correlated with electronic spin transition