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In the system Na 2 O-Al 2 O 3 -SiO 2 -H 2 O-TiO 2 , the behavior of Ti-containing structural complexes has been determined in H 2 O-saturated silicate melts and in coexisting silicate-saturated aqueous fluids as well as in silicate-rich supercritical fluids to 900 °C and 2225 MPa. Titanium speciation in aqueous fluids in the system TiO 2 -H 2 O was also characterized. All measurements were carried out in situ at the desired temperature and pressure using confocal microRaman and microFTIR spectroscopy. The experiments were carried out in an Ir-gasketed hydrothermal diamond-anvil cell (HDAC) with K-type thermocouples for temperature measurement and the Raman shift of  13 C synthetic diamond to monitor pressure.

High-pressure and high-temperature titanium solution mechanisms in silicate-saturated aqueous fluids and hydrous silicate melts