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The structure of phosphorus-bearing, H 2 O-saturated silicate melts, silicate-saturated aqueous fluids, and silicate-rich single phase (supercritical) liquids has been characterized in situ to 800 °C and 1486 MPa in an Ir-gasketed hydrothermal diamond-anvil cell (HDAC) with the aid of both confocal microRaman and FTIR spectroscopy. Temperature and pressure in the HDAC were recorded with thermocouples (±1 °C uncertainty) and pressure- and temperature-dependent Raman shift of  13 C diamonds (±40 MPa uncertainty). Starting materials were aluminum-free Na 2 O·4SiO 2  (NS4) and with 10 mol% Al 2 O 3  (NA10) substituting for SiO 2 , both with 5 mol% P 2 O 5 .

american mineralogist

Amorphous Materials. An experimental study of phosphorous and aluminosilicate speciation in and partitioning between aqueous fluids and silicate melts determined in-situ at high temperature and pressure