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The metatorbernite [Cu(UO 2 ) 2 (PO 4 ) 2 ·8H 2 O] structure comprises autunite-type sheets of cornersharing uranyl square bipyramids and phosphate tetrahedra, with the interlayer region occupied by Cu 2+  ions and molecular water. Previous studies have shown that heating induces stepwise dehydration and reduction in basal spacing. Structures of the lower hydrates have not been determined previously because suitable single crystals of these phases have yet to be prepared.

Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO 2 ) 2 (PO 4 ) 2 ·8H 2 O]