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An approximate low-temperature, metastable phase diagram is drawn for the system (1 - X) Fe 2 O 3 -(X)FeTiO 3 . It is based on published and new magnetic data from nine synthetic samples with bulk compositions in the range 0.6 &lt; X &lt; 1.0. Fields are plotted for (1) the paramagnetic phase (PM); the Fe 2 O 3 -rich ferrimagnetic phase (FM); (2) the FeTiO 3 -rich antiferromagnetic phase (AF); and (3) a re-entrant spin-glass phase (RSG). In addition, two subfields are plotted: (1) FM′, a subfield of the FM-phase, which occurs below a characteristic temperature TK, at which the magnetic susceptibility drops sharply on cooling, and (2) PM′, a subfield of the PM-phase (traditionally called superparamagnetic) forms below a sharp rise in susceptibility at TS, and exhibits measurable dispersion in the magnetic susceptibility at T &lt; TS.

A low-temperature phase diagram for ilmenite-rich compositions in the system Fe 2 O 3 -FeTiO 3