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A model for the modulated crystal structure of an antigorite polysome with m = 16 (where m is related to the number of tetrahedra spanning a wavelength along a) was refined by single-crystal synchrotron diffraction data in C2/m, using crystals coexisting with the m = 17 polysome from Val Malenco, Italy, which was previously determined structurally. Lattice parameters [a = 81.664(10), b = 9.255(5), c = 7.261(5) Å, β = 91.409(5)°] were determined using a single-crystal diffractometer equipped with an area detector at the Desy synchrotron (Hamburg). The structure was solved by direct methods, and the model refined using 19 222 symmetry-related reflections. The final R 4σ  factor was 0.0951, calculated for 7246 reflections.

The crystal structure of a second antigorite polysome (m = 16), by single-crystal synchrotron diffraction