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Quartz segregations in paragneisses from the Paleozoic basement of the North Patagonian Andes contain highly saline multiphase fluid inclusions with the rare daughter mineral ferropyrosmalite detected by Raman analysis, besides halite, sylvite, hematite, and/ or magnetite. During heating experiments, L-V homogenization occurs (256–515 °C), followed by halite dissolution (287–556 °C) and the dissolution of ferropyrosmalite at 550–581 °C. The latter phase transition triggers the growth of clinoamphibole crystals according to the following idealized reactions, written for potential end-members:

Ferropyrosmalite-bearing fluid inclusions in the North Patagonian Andes metasedimentary basement, Argentina: A record of regional metasomatism