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The crystal chemistry and thermal behavior of Fe-carpholite from the Pollino Massif have been investigated by a multi-method approach. A combination of optical microscopy, scanning electron microscopy, mRaman spectroscopy, thermal analysis, room-temperature single-crystal X‑ray diffraction, and high-temperature X‑ray powder diffraction was employed.

Crystal chemistry and thermal behavior of Fe-carpholite from the Pollino Massif, southern Italy