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X-ray computed microtomography (X-μCT) is applied here to investigate in a non-invasive way the three-dimensional (3D) spatial distribution of primary melt and fluid inclusions in garnets from the metapelitic enclaves of El Hoyazo and from the migmatites of Sierra Alpujata, Spain. Attention is focused on a particular case of inhomogeneous distribution of inclusions, characterized by inclusion-rich cores and almost inclusion-free rims (i.e., zonal arrangement), that has been previously investigated in detail only by means of 2D conventional methods. Different experimental X-μCT configurations, both synchrotron radiation- and X-ray tube-based, are employed to explore the limits of the technique. The internal features of the samples are successfully imaged, with spatial resolution down to a few micrometers.

Three-dimensional distribution of primary melt inclusions in garnets by X-ray microtomography