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Much interest has been devoted to dinuclear nickel(II) complexes with organic ligands because of their various structures deduced from the coordinating ability of the organic ligands. Previously, we reported on dinuclear nickel(II) complexes with organic ligands having donor atoms as bridging groups, which have the low-spin or high-spin nickel(II) state, resulting in a diamagnetic or paramagnetic property, respectively, depending on the donor atoms.1–7 In this study, we synthesized a new nickel(II) complex with N,N′-disalicylidene-2,2′-(ethylenedioxy)bis(ethylamine) (H2dee), and determined the crystal structure of the isolated complex, which shows a unique dinuclear core with twophenolato-oxygen bridges and the μ-aqua bridge, as shown in Fig. 1. The ligand H2dee was synthesized by a reaction of 2,2′-(ethylenedioxy)bis(ethylamine) with salicylaldehyde according to a method described in the literature.8 The complex was prepared by a 1:1 reaction of H2dde and nickel(II) salt in 2017 © The Japan Society for Analytical Chemistry

Di-μ-phenolato-μ-aqua-bridged Dinuclear Nickel(II) Complex with <i>N,N</i>′-Disalicylidene-2,2′-(ethylenedioxy)bis(ethylamine)