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The title compound, (CHP)(CHNOS)CuI.0.34HO, was obtained by the slow evaporation of a solvent from an acetonitrile solution containing a mixture of (PPh)N,N'-disulfobenzoquinonediimine and CuI. The structure consists of a one-dimensional metal-organic framework of the dianion and CuI. The anionic chains are surrounded by relatively large counter-cations, and are thus well isolated from each other

One-Dimensional Anionic Metal-Organic Chain Generated from (Tetraphenylphosphonium)<sub>2</sub>benzoquinonediiminedisulfonate and CuI