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The crystal structure of dimethyl 2-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)oxy]-2-butenedioate is monoclinic, space group P21/c with a = 7.9785(16), b = 24.801(6), c = 7.9550(16)A, β = 118.904(13)° and Z = 4. The crystal structure was solved by direct methods and refined by full-matrix least squares to final values of R1 = 0.0567 and wR2 = 0.0884 with 1927 reflections (I > 2 σ(I)).

Crystal Structure of Dimethyl 2-[(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)oxy]-2-butenedioate