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The structure of the title compound, [C26H29N2O5]·PF6·H2O (= [LH]·PF6·H2O), was confirmed by low-temperature single-crystal analysis. The crystal system belongs to triclinic with a space group of P1. The crystal structure reveals that the three-dimensional skeleton of [LH]+ adopts an approximate S-shape, and the intermolecular hydrogen bond between the quinoline nitrogen atoms of the adjacent molecules leads to form a helical 1-D polymer expanded along the b-axis.

Crystal Structure of [1,13-Bis(8-quinolyl)-1,4,7,10,13-pentaoxatridecanylprotonato]hexafluorophosphate monohydrate