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H2Co2P4O14 crystals were synthesized by a hydrothermal technique. They crystd. in a monoclinic system with cell parameters a 9.1609(7), b 12.6764(8), c 9.6868(10) A and I² 106.771(7)Â°. An open framework structure having tunnel-type cavities is obsd. [on SciFinder(R)]

Hydrothermal Synthesis and Structure of Dihydrated Cobalt Pyrophosphates