English (United Kingdom)

https://curated-unify.zendy.io/wp-json/zendy-region/v1/featured_content/oa?rat=en

https://curated-unify.zendy.io/wp-json/zendy-region/v1/highlighted_journal/

Global: Zendy Plus annual

Presents the access of premium content as premium feature

Premium Content

Presents the keyphrase highlighting as premium feature

Keyphrase Highlighting

Presents the summarisation as premium feature

Summarisation

Insights

Presents the pdf analysis as premium feature

PDF Analysis

Presents the zaia usage as premium feature

ZAIA

Global: Zendy Plus monthly

Global: Zendy Tools annual

Global: Zendy Tools monthly

Global: Zendy Free Plan

A simple and rapid solid phase extraction (SPE) procedure has been developed for the extraction and determination of uranium in water samples. The method is based upon the adsorption of uranium(VI)-2,3-dihydroxynaphthalene complex on microcrystalline naphthalene at the pH range 10 - 12 in the presence of a counter cation cetyltrimethylammonium ion. The solid mass consisting of uranium-2,3-dihydroxynaphthalene-CTA complex and naphthalene is ignited in the furnace at a temperature of 700°C for 1 h and then digested in dil. HNO 3 solution. Uranium is then determined by LED fluorimetry using fluorescence enhancing pyrophosphate buffer. The effects of different variables like pH of the solution, reagent concentrations, counter cations, stirring time, interfering ions etc. have been investigated thoroughly for the quantitative recovery of uranium. The accuracy of the developed method has been ascertained by standard addition method as well as conventional pellet fluorimetry method involving co-precipitation of uranium using aluminum phosphate as a carrier.

analytical sciences

Separation and Preconcentration of Trace Uranium(VI) by Solid Phase Extraction with 2,3-Dihydroxynaphthalene and Cetyltrimethylammonium Bromide on Molten Naphthalene and Its LED Fluorimetric Determination in Water Samples