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Attenuated total reflectance-far ultraviolet (ATR-FUV) spectra of Li + and polyether ligands, such as glymes and poly (ethylene glycol) (PEG), in solution give information about changes in the electronic states of the ligands. From the ATR-FUV spectra, the coordination numbers between Li + and monoglyme, diglyme, triglyme, and PEG400 were determined to be 4, 5, 6, and 5, respectively. Our results indicate that Li + is coordinated only by the ligands rather than its counter-ions.

analytical sciences

Determining the Coordination Number of Li+ and Glyme or Poly(ethylene glycol) in Solution Using Attenuated Total Reflectance-Far Ultraviolet Spectroscopy