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We successfully synthesized a garnet-type Li6.5La3Zr1.5Ta0.5O12 polycrystalline sample at a relatively low temperature of 700°C using pyrochlore-type La2Zr2O7 and weberite-type La3TaO7 as precursor oxides. The cubic garnet-type structure with the lattice parameter of a = 1.29577(1) nm was confirmed using powder X-ray diffraction data. The primary particle size of the present Li6.5La3Zr1.5Ta0.5O12 sample was about 2 ̄m, which is considerably smaller than that prepared using conventional solid-state reaction at higher temperatures. Thermogravimetry differential thermal analysis data confirmed that the reaction between LiOH·H2O and precursor oxides occurred above 500°C after the dehydration reaction of LiOH·H2O. ©2019 The Ceramic Society of Japan. All rights reserved.

journal of the ceramic society of japan

A novel synthetic route of garnet-type Li&lt;sub&gt;6.5&lt;/sub&gt;La&lt;sub&gt;3&lt;/sub&gt;Zr&lt;sub&gt;1.5&lt;/sub&gt;Ta&lt;sub&gt;0.5&lt;/sub&gt;O&lt;sub&gt;12&lt;/sub&gt; using pyrochlore-type La&lt;sub&gt;2&lt;/sub&gt;Zr&lt;sub&gt;2&lt;/sub&gt;O&lt;sub&gt;7&lt;/sub&gt; and weberite-type La&lt;sub&gt;3&lt;/sub&gt;TaO&lt;sub&gt;7&lt;/sub&gt; as starting materials