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*Department of Applied Chemistry, School of Science and Engineering, Waseda University, 3–4–1 Ohkubo, Sinjuku-ku, Tokyo 169–8555, Japan **Kagami Memorial Research Institute for Materials Science and Technology, Waseda University, 2–8–26 Nishiwaseda, Shinjuku-ku, Tokyo 169–0051, Japan ***Institut Charles Gerhardt, Chimie Moléculaire et Organisation du Solide, Université de Montpellier, cc 1701. Place E. Bataillon, 34095 Montpellier Cedex 5, France

Intercalation of <i>n</i>-alkylamines and alkylene diamines into carboxyl functionalized lamellar-type silsesquioxane