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The low-temperature carbothermal nitridaton of boron oxide (B2O3) was induced by the networked carbon structure prepared from a condensed boric acid (H3BO3)-poly(vinyl alcohol) (PVA) product. The precursor powder consisting of B2O3 and carbon components was formed from the condensed product by thermal decomposition in air, and heated at 1200°C in a N2 flow. The formation of boron nitride (BN) was accelerated for the product obtained from the precursor powder with the networked carbon structure. The formation of boron carbide (B4C) by carbothermal reduction was also observed, and the formed B4C was converted into BN with further increasing heat treatment time.

Low-temperature carbothermal nitridation of boron oxide induced by networked carbon structure