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We studied a means of synthesizing colloidal nanocrystals (NCs) of ¢-LiGaO2, a wide-band gap semiconductor oxide, by reacting lithium hydroxide (LiOH) with gallium tri-iso-propoxide [Ga(OiPr)3] in benzylamine. This reaction yielded near-stoichiometric ¢-LiGaO2 NCs, 4­5nm in diameter and capped with n-octylamine, which were highly dispersible in an organic solvent. We proposed that the LiOH and Ga(OiPr)3 reacted via electrophilic attack of Li on the bridging oxygen of Ga(OiPr)3 and/or nucleophilic attack of OH on the ¡-carbon of Ga(OiPr)3. This reaction formed Li­O­Ga bonds and contributed to the nearstoichiometry of the resultant ¢-LiGaO2 NCs. ©2014 The Ceramic Society of Japan. All rights reserved.

Synthesis of colloidal solution of β-LiGaO<sub>2</sub> nanocrystals capped with organic surfactant