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We have investigated the effect of the Ca/P molar ratio in the starting composition on the synthesis of octacalcium phosphate intercalated with dicarboxylate ions (OCPC), starting from calcium carbonate and phosphoric acid in the presence of a dicarboxylic acid, such as succinic acid, adipic acid, or suberic acid. For a Ca/P molar ratio in the starting composition of 1.6, which is the stoichiometric value for OCPC, the highest yield of OCPC with a high degree of crystallinity was obtained for the OCPC samples synthesized with starting Ca/P molar ratios of 1.5, 1.6, and 1.7. The Ca/P molar ratio of the starting composition is an important factor in the synthesis of OCPC. This synthesis route provides for the effective production of OCPC samples.

Synthesis of octacalcium phosphate intercalated with dicarboxylate ions from calcium carbonate and phosphoric acid