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A new method has been developed to determine in-situ the oxygen content in the superconducting Ba2YCu3Ox phase in equilibrium with the oxygen atmosphere from 0.2 to 10atm. The oxygen content was determined by the pressure change in a closed system due to the oxygen evolution from the sample at room temperature and high temperature, The results obtained at the lower pressure showed a good agreement with those determined by other methods. Ba2YCu3Ox absorbed some amount of oxygen during cooling in spite of a high cooling rate for the high pressures of oxygen

nihon seramikkusu kyoukai gakujyutsu rombunshi/nippon seramikkusu kyōkai gakujutsu rombunshi

Determination of Oxygen Content in Ba&lt;sub&gt;2&lt;/sub&gt;YCu&lt;sub&gt;3&lt;/sub&gt;O&lt;sub&gt;&lt;i&gt;x&lt;/i&gt;&lt;/sub&gt; in Equilibrium with Oxygen Pressure of 0.2-10atm