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The effects of the hydrated alumina film obtained from hydration process on the porous anodic alumina (PAA) film fabricated under the ultrahigh voltage in a mixed electrolyte were investigated. It is found that the hydrated alumina film can enhance the voltage of anodization and facilitate the uniform growth of the PAA film. The suitable thickness of the hydrated alumina film can be used to facilitate the selfassembly formation of the unite cell on porous PAA film. Besides, it is found that some of aluminum nanocones is presented on the sidewalls of the nanodents, due to the relatively poor self-assembly of the nano-structural units, which result in the inadequacy transformation of the aluminum between the nanostructural units to the alumina. These finding may can be used for fabricating the aluminum nanostructure on the aluminum surface directly.

Effect of Hydration on Porous Anodic Alumina with Large Interpore Distances during Anodization with Ultrahigh Voltage