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A molecularly imprinted electrochemical sensor was developed for the detection of pefloxacin. The molecularly imprinted polymer (MIP) was prepared via electrodeposition on the surface of a gold nanoparticles/reduced graphene oxide/single-walled carbon nanotubes modified glass carbon electrode by incorporation of pefloxacin as a template molecule during the electrochemical polymerization of ophenylenediamine. The namocomposite of gold nanoparticals/reduced graphene oxide/single-walled carbon nanotubes was obtained by one-step electrochemical reduction. Differential pulse voltammogram (DPV) showed a linear pefloxacin concentration range from 5.0 × 10 mol/L to 2.0 × 10 mol/L, and the detection limit was 1.6 × 10 mol/L. The sensor also showed high selectivity, stability and reproducibility. Moreover, the sensor was successfully applied in the analysis of actual milk samples with satisfactory recovery rates.

international journal of electrochemical science

A novel Molecularly Imprinted Sensor based on Gold Nanoparticles/Reduced Graphene Oxide/Single-Walled Carbon Nanotubes Nanocomposite for the Detection of pefloxacin