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Co–Ni–Fe thin films electrodeposited by a rectangular pulse current technique within a frequency range from 0.1 to 1.2 MHz were investigated using energy dispersive X-ray microscopy and X-ray diffraction. The Fe, Ni, and Co contents in the Co–Ni–Fe films rapidly increased at resonant frequencies. The number of resonant frequencies was odd, and was explained by an energy-level transition. With an increase in the Fe content, the crystal structures of the Co–Ni–Fe thin films changed from the hexagonal closed-packed (HCP) crystal structure, to an amorphous structure, and further to the body-centered cubic (BCC) crystal structure.

international journal of electrochemical science

Resonant Change in Element Contents and Crystal Structure Change in Co–Ni–Fe Thin Films Electrodeposited Using Rectangular Pulse Current over Megahertz Frequency Range