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Using cyclic voltammetry, Raman scattering and infrared (IR) spectroscopy, new findings concerning the electrochemical synthesis of composites based on multi-wall carbon nanotubes (MWNTs) and polypyrrole (PPY) doped with H3PMo12O40 heteropolyanions are described in this report. To better understand the electrochemical mechanism behind the synthesis of these composites, the influence of the concentrations of pyrrole and the electrolytes of H3PMo12O40 and H2SO4 on the cyclic voltammogram profile is studied. The formation of PPY doped with H3PMo12O40 heteropolyanions onto the MWNT surface is demonstrated by complementary studies of Raman scattering and IR spectroscopy.

international journal of electrochemical science

Electrochemical Synthesis of the Composites Based on Multi-Wall Carbon Nanotubes and Polypyrrole Doped with Phosphomolybdic Acid Heteropolyanions and Their Vibrational Properties