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In this paper, a composite electrolyte of (Na/K)Ti2(PO4)3/Ti0.9Mg0.1P2O7 was synthesized using Ti0.9Mg0.1P2O7 and NaCl/KCl as raw materials. The composite electrolyte was characterized with XRD, SEM and EIS. The result of X–ray diffraction (XRD) indicated that an in-situ reaction fully occurred to Mg-doped titanium pyrophosphate and inorganic molten salt to form the Ti0.9Mg0.1P2O7 and (Na/K)Ti2(PO4)3 bimorph structure. It can be seen from scanning electron microscopy (SEM) images that Ti0.9Mg0.1P2O7 and (Na/K)Ti2(PO4)3 are fused each other. The electrical conductivities results by electrochemical impedance spectroscopy (EIS) indicated that the (Na/K)Ti2(PO4)3/Ti0.9Mg0.1P2O7 shows a greatly improvement of conductivities. Finally, an H2/O2 fuel cell employing Ti0.9Mg0.1P2O7/(Na/K)Ti2(PO4)3 as electrolyte was fabricated.

Intermediate Temperature Electrical Properties of a (Na/K)Ti2(PO4)3/Ti0.9Mg0.1P2O7 Composite Electrolyte