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A powder microelectrode (PME), embedded with Nafion-carboxyl multiwalled carbon nanotubes (MWCNTs), was prepared for selective and sensitive determination of sulfonamides. The effects of experimental parameters on the response of electrode such as pH of buffer, scan rate were optimized. Under optimal conditions, the proposed PME can greatly improve the determination sensitivity. In a Britton-Robison (BR) buffer solution (pH 2.0), the linear response range for detection of 1.0×10 -5

Two-electrode Sensor System for Rapid Detection of Sulfonamides by Applying the Nafion-Carboxyl Multiwalled Carbon Nanotubes Powder Microelectrode