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Ni, Fe and Ni-Fe alloys electrodeposition were tested in two ionic liquids. The first one is a commercial (1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide ([P1,4][Tf2N])) and the second is a homemade (tri(n-butyl)[2-ethoxy-2oxoethyl]ammonium bis (trifluoromethylsulfonyl)imide([BuGBOEt][Tf2N])). Covering iron deposits was obtained in the [BuGBOEt][Tf2N]. Nickel deposition was only possible in the [P1,4][Tf2N]. Ni-Fe alloys were obtained from the [P1,4][Tf2N] solvent. The study of the evolution of alloys composition versus polarisation shows irregular evolution depending on the applied potential. The alloys composition varies approximately between Ni70-Fe30 and Ni90-Fe10 for applied potentials including to 1.8 V and 4 V versus Ni electrode. The chemical composition, the surface morphology and the structure, of deposits were characterized by scanning electron microscopy (SEM), energy dispersive analysis (EDX) and Xray diffraction (XRD).

international journal of electrochemical science

Electrodeposition of Ni, Fe and Ni-Fe Alloys in Two Ionic Liquids: (tri (n-butyl) [2-methoxy-2-oxoethyl] Ammonium bis (trifluoromethylsulfonyl) [BuGBOEt] [Tf2N] and (1-butyl-1-methylpyrrolidinium bis trifluoromethylsulfonyl) imide ([P1,4] [Tf2N])