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Substitution reaction of hydroxy of citronellol with chloride using a mixture of ammonium chloride (NH 4 Cl) and sulphuric acid (H 2 SO 4 ) has been conducted. The citronellol was obtained from the reduction of citronellal using sodium borohydride (NaBH 4 ) at room temperature for 30 minutes. Substitution of hydroxy of citronellol with chloride ion was carried out at 80 o C and molarity ratio of citronellol and NH 4 Cl 1:1, 1:2; 1:3; and 1:4 respectively. Identification of the product by gas chromatography-mass spectrometry (GC-MS) showed that the substitution reaction produced 2-isopropyl-5-methyl-1-chlorocyclohexane compound with rendemen 64,49 % in mol ratio of 1:4. The infra red (IR) analysis showed that there was a vibration at wave number 763 cm -1 which is a typical C-Cl vibrations.

SUBSTITUTION REACTION OF HYDROXY OF CITRONELLOL WITH CHLORIDE USING A MIXTURE OF AMMONIUM CHLORIDE AND SULPHURIC ACID