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Transition metal complexes of Cu(II) and Ni(II) with 2-benzoylpyridinesemicarbazide hydrochloride with general composition ML2X2 (where M= Cu(II) and Ni(II), L= 2-benzoypyridine and semicarbazide hydrochloride ligand, X= Cl ,NO3 , SO4 2, OAc have been synthesised and characterised by elemental analysis, magnetic moment, conductivity measurement, mass spectrometry, IR spectrometry, UV-Vis spectroscopy, and EPR spectral studies. The magnetic moment values indicate that these are high spin complexes. The IR spectral study indicates that ligand is bidentate and coordinated through N and O. On the basis of spectral study Octahedral geometry was proposed for Ni(II) complexes and tetragonal geometry was proposed for Cu(II) complexes.

international journal of therapeutic applications

SPECTROSCOPIC STUDY AND SYNTHESIS OF SCHIFF’S BASE LIGAND OF 2-BENZOYLPYRIDINE SEMICARBAZIDE HYDROCHLORIDE AND ITS Cu(II) AND Ni(II) TRANSITION METAL COMPLEXES