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samples at levels between 0.025 and 0.075 µg kg –1 were 99.6–110.3% with precision of 10.5–13.4%, confirming the immunochemical method precision and reliability for intensive surveillance studies. According to the regulatory requirements, for confirmation of the obtained positives from the screening, the reference high-performance liquid chromatographic procedure was evaluated in reference to the performance criteria. The between-day recovery obtained was in the range 67.2–72.8%, and the precision range was 5.4–9.1%. Two hundred and twenty five positives from the screening were subjected to confirmatory analysis. Comparison of the data obtained from the immunoassay and chromatographic method (R 2 = 0.764) revealed a slight overestimation of the screening method, but no cases of false-negative de

macedonian journal of chemistry and chemical engineering

Study on the method performances for screening and confirmatory analysis of aflatoxin M1 in raw milk according to the mycotoxin regulative requirements