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The conditions of successful iron-carbon coupling in the reaction between cyclopentadienyliron dicarbonyl iodide and methyl propiolate upon the Pd/Cu catalysis were determined. A new high-yield synthetic approach to the methoxycarbonylethynyl iron complex Cp(CO)2Fe-C≡C-COOMe were developed.

Pd/Cu-Catalyzed Coupling of Cyclopentadienyliron Dicarbonyl Iodide and Methyl Propiolate in Synthesis of Cp(CO)₂Fe-C≡C-COOMe