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Ru compacts with mean grain size of 4~5 μm were prepared by vacuum hot pressing (VHP), and the compacts with the maximum density of 12.2 g/cm was obtained with sintering time of 2 h. X-ray diffractometer (XRD) revealed that there was a texture change with sintering time. The microstructure of Ru compacts was observed by electron backscatter diffraction (EBSD) and field emission scanning electron microscope (FSEM). Thus, the microstructure evolution with sintering time were discussed.

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Microstructure Evolution of Ruthenium During Vacuum Hot Pressing : Obtaining fine-grained metal with mechanical properties close to electron-beam melted ruthenium