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(NH4)2CO3 as absorbing solution and 5 min of reflux. Temperature during combustion was higher than 1400 °C and the residual carbon content in digest obtained after MIC was lower than 1%. Up to eight samples could be processed simultaneously and a single absorbing solution was suitable for both Br and Cl. Limit of quantification by MIC and further ICP OES determination was 12 and 6 µg g -1 for Br and Cl, respectively.

journal of the brazilian chemical society

Bromine and chlorine determination in cigarette tobacco using microwave-induced combustion and inductively coupled plasma optical emission spectrometry