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B(HSO4)3 was easily prepared and used as a novel and efficient solid acid catalyst for conversion of epoxides to the corresponding thiocyanohydrins under solvent-free conditions with high isolated yields. The salient features of this methodology are cheaper process, easy availability of the catalyst, versatility, and high regioselectivity of the procedure.

B(HSO4)3: a novel and efficient solid acid catalyst for the regioselective conversion of epoxides to thiocyanohydrins under solvent-free conditions