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N,N,N',N'-tetrabromo-benzene-1,3-disulfonylamide [TBBDA] was reacted with semicarbazones and converts them to their corresponding carbonyl compounds in excellent yields under solvent-free conditions.

Facile and mild deprotection of semicarbazones under solvent-free conditions with N,N,N',N'-tetrabromo-benzene-1,3-disulfonylamide