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A new pentacoordinate Sn (IV) adduct was prepared from diphenyltin (IV) dichloride and the disulphoxide 2-phenyl-1,3-dithiane trans-1, trans-3-dioxide. Spectroscopic and X-ray diffraction studies showed the new compound to be a rare example of a pentacoordinate 1:1 adduct between an organometallic Sn (IV) species and a neutral ligand. In spite of being difunctional, the ligand is monodentate as a result of its peculiar geometry. Moreover, the adduct does not show any evidence of strong intermolecular interactions, forming discrete molecules.

journal of the brazilian chemical society

Adduct formation between diphenyltin dichloride and 2-phenyl-1,3-dithiane trans-1-trans-3-dioxide: preparation, spectroscopy, crystal and molecular structure of Ph2SnCl2.CH2(CH2)2SOCH(Ph)SO