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This study proposes a method of direct and simultaneous determination of the amount of Ca2+ and Mg2+ present in soil extracts using a Calcium Ion-Selective Electrode and by Complexometric Titration (ISE-CT). The results were compared to those obtained by conventional analytical techniques of Complexometric Titration (CT) and Flame Atomic Absorption Spectrometry (FAAS). There were no significant differences in the determination of Ca2+ and Mg2+ in comparison with CT and FAAS, at a 95 % confidence level. Additionally, results of this method were more precise and accurate than of the Interlaboratorial Control (IC). Neste trabalho foi proposto um método para determinar de forma direta e simultânea a quantidade de Ca2+ e Mg2+ trocáveis presente em extratos de solos, empregando-se eletrodo íon seletivo de Ca e titulação complexométrica (EIS-TC). Os resultados dessas determinações foram comparados aos dados obtidos por meio de técnicas analíticas convencionais de Titulação Complexométrica (TC) e Espectrometria de Absorção Atômica com Chama (FAAS). Não houve diferenças significativas nas determinações dos íons Ca2+ e Mg2+ em relação aos métodos TC e FAAS, com 95 % de confiança. Adicionalmente, o método apresentou melhor precisão e exatidão quando seus resultados foram comparados aos do Controle Interlaboratorial (CI)

Complexometric titration with potenciometric indicator to determination of calcium and magnesium in soil extracts¹