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We have developed a method to determine anilines derived from pesticides by high performance liquid chromatography with an electrochemical detector. Pesticides were hydrolyzed with HCl or KOH to the corresponding anilines, which were isolated from the hydrolysates by steam distillation/solvent extraction. Quantitative determinations were done by reversephase high performance liquid chromatography without derivatization. Anilines in subnanogram quantities were detected with an electrochemical detector. Recovery data were obtained from egg plant samples fortified with fluoroimide, aniliazine, linuron, alachlor or iprodione at 0.4ppm. Average recoveries for fluoroimide, anilazine, linuron, alachlor and iprodione were 100, 85, 68, 27 and 89%, respectively.

Determination of Aniline Compounds by High Performance Liquid Chromatograph with an Electrochemical Detector